Thermo Scientific Orion VERSA STAR pH ISE Temperature

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Ross and the COIL trade dress are trademarks of Thermo Fisher Scientific Inc and. its subsidiaries, AQUAfast AQUASensors BOD AutoEZ ionplus KNIpHE LogR No Cal ORION perpHect. PerpHecT pHISA pHuture Pure Water Sage ROSS ROSS Ultra Sure Flow Titrator PLUS and. TURBO2 are registered trademarks of Thermo Fisher Scientific Inc and its subsidiaries. A All in One Aplus AUTO BAR AUTO CAL Auto ID AUTO READ AUTO STIR. Auto Test AutoTration CISA digital LogR DuraProbe EZ Startup ISEasy. Low Maintenance Triode Minimum Stir Requirement MSR NISS Optimum Results Orion Dual. Star Orion Star SAOB SMART AVERAGING SMART STABILITY Star LogR Star Navigator 21. Stat Face Triode are trademarks of Thermo Fisher Scientific Inc and its subsidiaries. Guaranteed Success and The Technical Edge are service marks of Thermo Fisher Scientific Inc. and its subsidiaries, 2011 Thermo Fisher Scientific Inc All rights reserved All trademarks are the property of. Thermo Fisher Scientific Inc and its subsidiaries, The specifications descriptions drawings ordering information and part numbers within this. document are subject to change without notice, This publication supersedes all previous publications on this subject. Thermo Scientific Orion VERSA STAR pH ISE Temperature Module. Table of Contents,Chapter 1 Introduction 1,Chapter 2 Module Overview 3.
Module Connections and Inputs 3,Module Maintenance 4. Display Information From Module 4,Chapter 3 Setup Menus 5. Setup Menus for Primary Measurements 5,Read Type Information 6. Isopotential Value 7,Linear Regression Information 7. Low Level Stability 7,Setup Menu for Temperature 7.
Chapter 4 pH RmV and ORP Calibration 9,pH Calibration 9. RmV Calibration 9,ORP Calibration 10,Chapter 5 ISE Calibration 11. Chapter 6 Temperature Calibration 13,Chapter 7 Measurement 15. pH mV RmV ORP Measurement 15,ISE Measurement 15,Chapter 8 Methods 17. Chapter 9 Incremental Techniques 19,Known Addition and Subtraction 19.
Single Known Addition 20,Double Known Addition 20,Single Known Subtraction 21. Double Known Subtraction 21,Analyte Addition and Subtraction 22. To Access Incremental Techniques 22,Chapter 10 Data Storage and Review 23. Data Storage Settings 23,Measurement Read Type 23,Datalog Computer and Printer Export Settings 23. Datalog Review 23,Calibration Review 24,Chapter 11 Customer Services 25.
Troubleshooting Guide 25,Assistance 25,Warranty and Registration 25. WEEE Compliance 25,Declaration of Conformity 26,pH ISE Temperature Module Specifications 27. Ordering Information 28,Appendix Advanced Features 33. Automatic pH Buffer Recognition Feature 33, Testing a pH Electrode for Automatic Buffer Recognition 33. pH Electrode Condition Icon 34,Multipoint Calibration Curve Feature 35.
Automatic Blank Non Linear Correction Feature 36,Determining an Isopotential Value 37. Chapter 1 Introduction, Thank you for your purchase of the Thermo Scientific Orion VERSA STAR pH ISE Temperature Module. This module is for use with the Thermo Scientific Orion VERSA STAR Advanced Electrochemistry Benchtop Meter. Some key features of this module include, pH range from 2 to 20 with resolution options of 0 001 0 01 and 0 1. ISE range from 0 to 19999 with resolution of up to four significant digits. mV and RmV ranges from 2000 mV,Automatic and manual datalogging options. Up to 6 point pH calibration with automatic recognition for USA NIST and DIN buffers. Up to 6 point ISE calibration with adjustable ISO point capabilities. The ability to fix pH ISE calibration errors without a complete recalibration thanks to calibration editing. Advanced ISE features such as auto blank timed end point linear point to point non linear selectable. auto blank low concentration range stability ISE ID and incremental techniques. Please read this reference guide thoroughly Any use outside of these instructions may invalidate your warranty and. cause permanent damage to the meter, Thermo Scientific Orion VERSA STAR pH ISE Temperature Module 1.
This page intentionally left blank,Chapter 2 Module Overview. To connect the modules to the meter and for specific information regarding the meter outputs please see the. Orion VERSA STAR Reference Guide The Reference Guide is on the CD included with the meter and also available. at www thermoscientific com water,Module Connections and Inputs. The Orion VERSA STAR meter can accept Orion combination ISE electrodes as well as separate reference and sensing. half cell electrodes This allows for a wider ISE measurement offering Half cell electrodes separate the ions sensing. from the reference electrode For difficult samples the flexibility of using alternate fill solutions may be an advantage. to researchers, 1 Prepare the pH or ISE electrode and ATC probe for use as instructed in the electrode user guides. The pin tip reference connector is on the lowest panel of the pH ISE module. 2 Place the pH or ISE ATC probe and Orion Star stirrer probe cat no 096019 optional into the. electrode arm, 3 Attach the pH or ISE BNC and ATC probe to the pH ISE meter module Lower ISE and ATC into. solution for conditioning if required If using the stirrer probe attach probe to the meter place into the. electrode arm and assign the probe to the channel in the setup menu for instrument settings. 4 Prepare fresh standards daily for calibration For ISE testing standards should be at least one decade. 10 times apart The standards should exceed the expected minimum and maximum sample range. Serial dilution is recommended using calibrated pipettes to accurately prepare calibration standards. from a stock solution,5 Gather reagents rinse water and other supplies.
For ISE testing if ISA will be added to the sample it needs to be added to all the standards prior to. calibration to ensure a consistent dilution factor. pH ISE Module,8 pin mini DIN for ATC,BNC connection with shorting cap. Reference pin socket, Thermo Scientific Orion VERSA STAR pH ISE Temperature Module 3. Module Maintenance, For routine maintenance dust and wipe the module with a damp cloth If necessary warm water or mild water based. detergent can be used Maintenance can be performed on a daily weekly or monthly basis as required by operating. environment Immediately remove any spilled substance using the proper cleaning procedure for that spill type. Display Information from Module,Example ISE Measurement Screen Single Channel. Date and time,Primary reading,Corresponding,Calibration.
information,The information on the display can be customized. Enter the setup menu to make changes,1 Press Setup. 2 Use the arrow keys to highlight Inst Settings,press f3 select key. 3 Use the arrow key to highlight Display View,Press f3 select key. 4 Follow the onscreen prompts to choose what you,would like to see on the measurement screen.
4 Thermo Scientific Orion VERSA STAR pH ISE Temperature Module. Chapter 3 Setup Menus,Setup Menus for Primary Measurements. 1 Press Setup f3 to access the Main Setup Screen, 2 Use the arrow key to scroll across to the modules to ISE channel you wish to use and. press Select f3, 3 Scroll to across to the mode menu and press Select f3. ISE Setup Menu,Default values are in bold in the table below. Electrode Serial Number Input,Electrode Type See table below.
Sample ID Off Manual Auto Increment,Significant Digits 1 2 3 4 digits. Stability Smart Fast Medium Slow,Averaging Off Automatic Smart. Read Type AutoRead Timed Continuous,Measure Unit ppm Molar mg L ppb None. Isopotential Value Off On,Linear Regression Off On. Blank Correction Off On,Low Level Stability Off On.
Alarm Limit CalDue Set Point,Limit and set point alarm default set to off. Cal due alarm set to 12 hours,pH Setup Menu,Default values are in bold in the table below. Electrode ID Input,Sample ID Off Manual Auto Increment. Resolution 0 1 0 01 0 001,Stability Smart Fast Medium Slow. Averaging Off Automatic Smart,Read Type AutoRead Timed Continuous.
Buffer Group USA DIN Custom,Isopotential Value Off On 7 000. Linear Regression Off On,Alarm Limit CalDue Set Point. Limit and set point alarm default set to off,Cal due alarm set to 12 hours. Thermo Scientific Orion VERSA STAR pH ISE Temperature Module 5. ORP RmV and mV Setup Menus,Default values are in bold in the table below. Electrode ID Input,Sample ID Off Manual Auto Increment.
Resolution 1 0 0 1,Stability Smart Fast Medium Slow. Averaging Off Automatic Smart,Read Type AutoRead Timed Continuous. Alarm Limit CalDue Set Point,Only for ORP and RmV modes. Limit and set point alarm default set to off,Cal due alarm set to 12 hours. 4 For ISE testing select the ISE electrode being used in setup If your electrode is not listed. use the X electrode with the valence 1 2 1 or 2 matching your electrode for. accurate results,Ag I X CO2 REDOX ORP Cl2 S 2 ClO4 O2.
Cd 2 NH3 BF 4 K X 2 Cu 2 X F SCN,CN Pb 2 Cl NO3 Br NOx Ca 2 Na X 2. Read Type Information, There are three main read types available as shown in the setup menus. Auto Read The meter will display the measurement as it stabilizes and lock and hold the. measurement when it is stable The AR icon will lock on the screen Once the measurement is locked. the meter will automatically export the measurement to the data log if the data log is enabled in. the setup menu and to a printer or computer if a printer or computer is connected to the meter and. enabled in the setup menu To take a new measurement press measure esc 1. Timed The meter will read and display a measurement at the set time interval that is programmed. by the operator There are two options, 1 By checking selecting the Interval box at the set time interval the meter will automatically. export the measurement to the data log if the data log is enabled in the setup menu and to. a printer or computer if a printer or computer is connected to the meter and enabled in the. setup menu If selected enter the time interval value in a hours minutes seconds format using. the numeric keypad and press f3 select key, 2 If the Interval box is unchecked not selected a single timed measurement will be taken. The meter will apply the same saving and exporting conditions as with the set time interval to. record and export data but lock after one timed interval has expired Press measure esc 1 to. reset the countdown clock and take a new reading, 6 Thermo Scientific Orion VERSA STAR pH ISE Temperature Module.
Continuous The meter will continuously measure and update the display This read type is useful. when performing an experiment that requires continuous measurements to be taken Press the. log print 0 print key to export the measurement to the data log if the data log is enabled in the setup. menu and to a printer or computer if a printer or computer is connected to the meter and enabled in. Isopotential Value, The slope of all electrodes changes with temperature based on the Nerst equation The slope curves at the different. temperatures intersect at the isopotential value which is the concentration at which the potential of the electrode does. not vary with temperature For glass pH electrodes this value is 7 00 For other ion selective electrodes ISEs if the. isopotential value is known or can be measured experimentally adjusting this value makes temperature compensation. for an ISE possible Temperature compensation can be performed for one and two point calibrations. Linear Regression Information, The default is off which uses the traditional segmented approach The segmented approach is the most accurate and. precise More information can be found in the appendix section of this reference guide under the Multipoint Calibration. Curve Feature, Selecting on for this option results in the use of a single best fit line for the calibration curve and can be beneficial if. pH measurements vary greatly,Low Level Stability, This feature adjusts the timing for the calibration points for lower level ISE standards. Setup Menu for Temperature, All of the temperature measurement settings are found in Temperature Setup menu for each measurement.
Temperature Unit C or F selection, Temperature Input and Type Ch 1 ATC Ch 2 ATC Ch 3 ATC Ch 4 ATC MTC. Ch 1 ATC only or All ATC allows all ATCs to be,Temperature Cal. calibrated at once, This number will change to match the setup menu channel. Temperature probes can be set up in the measurement mode of the sample you are measuring Ch 1 ATC allows the. temperature probe to be used in more than one channel for temperature compensated measurements such as when. a pH electrode and a 2 cell conductivity cell are in the same measurement sample Temperature is a critical pH and. conductivity measurement as the measurement values require a temperature correction to determine the reference. value often 25 C in the America and 20 C in Europe. Thermo Scientific Orion VERSA STAR pH ISE Temperature Module 7. This page intentionally left blank, 8 Thermo Scientific Orion VERSA STAR pH ISE Temperature Module. Chapter 4 pH RmV and ORP Calibration,pH Calibration.
Up to six pH buffers can be used for calibration This can be a combination of automatically recognized USA NIST or. DIN buffer values and custom buffers Always use fresh pH buffers and select buffers that bracket the sample pH and. Thermo Scientific Orion VERSA STAR pH ISE Temperature Module 1 Chapter 1 Introduction Thank you for your purchase of the Thermo Scientific Orion VERSA STAR pH ISE Temperature Module This module is for use with the Thermo Scientific Orion VERSA STAR Advanced Electrochemistry Benchtop Meter Some key features of this module include

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